Battery Degradation Papers

 

A full list of publications to from the Degradation project to October 2023 can be found here.

  1. Structure-property insights into nanostructured electrodes for Li-ion batteries from local structural and diffusional probes; Laveda, J.V.; Johnston, B.; Paterson, G.W.; Baker, P.J.; Tucker, M.G.; Playford, H.Y.; Jensen, K.M.O.; Billinge, S.J.L.; Corr, S.A.; Journal of Materials Chemistry A (Dec 2017) https://doi.org/10.1039/c7ta04400c  
  2. In-Situ Electrochemical SHINERS Investigation of SEI Composition on Carbon-Coated Zn0.9Fe0.1O Anode for Lithium-Ion Batteries; Cabo-Fernandez, L.; Bresser, D.; Braga, F.; Passerini, S.; Hardwick, L.J.; Batteries and Supercaps (Sept 2018) https://doi.org/10.1002/batt.201800063  
  3. Evolution of electrochemical cell designs for in-situ and operando 3D characterization; Tan, C.; Daemi, S.R.; Taiwo, O.O.; Heenan, T.M.M.; Brett, D.J.L.; Shearing, P.R.; Materials (Nov 2018) https://doi.org/10.3390/ma11112157  
  4. Partially Neutralized Polyacrylic Acid/Poly(vinyl alcohol) Blends as Effective Binders for High-Performance Silicon Anodes in Lithium-Ion Batteries; Huang, Q.; Wan, C.; Loveridge, M.; Bhagat, R.; ACS Applied Energy Materials (Nov 2018) https://doi.org/10.1021/acsaem.8b01277 
  5. 4D visualisation of: In situ nano-compression of Li-ion cathode materials to mimic early stage calendering; Daemi, S.R.; Lu, X.; Sykes, D.; Behnsen, J.; Tan, C.; Palacios-Padros, A.; Cookson, J.; Petrucco, E.; Withers, P.J.; Brett, D.J.L.; Shearing, P.R.; Materials Horizons (Dec 2018) https://doi.org/10.1039/c8mh01533c (See also MSM)  
  6. Three-dimensional pulsed field gradient NMR measurements of self-diffusion in anisotropic materials for energy storage applications; Engelke, S.; Marbella, L.E.; Trease, N.M.; De Volder, M.; Grey, C.P.; Physical Chemistry Chemical Physics (Jan 2019) https://doi.org/10.1039/c8cp07776b  
  7. Modelling and experiments to identify high-risk failure scenarios for testing the safety of lithium-ion cells; Finegan, D.P.; Darst, J.; Walker, W.; Li, Q.; Yang, C.; Jervis, R.; Heenan, T.M.M.; Hack, J.; Thomas, J.C.; Rack, A.; Brett, D.J.L.; Shearing, P.R.; Keyser, M.; Darcy, E.; Journal of Power Sources (March 2019) https://doi.org/10.1016/j.jpowsour.2019.01.077  
  8. Evolution of Structure and Lithium Dynamics in LiNi0.8Mn0.1Co0.1O2 (NMC811) Cathodes during Electrochemical Cycling; Märker, K.; Reeves, P.J.; Xu, C.; Griffith, K.J.; Grey, C.P.; Chemistry of Materials (March 2019) https://doi.org/10.1021/acs.chemmater.9b00140  
  9. Temperature Considerations for Charging Li-Ion Batteries: Inductive versus Mains Charging Modes for Portable Electronic Devices; Loveridge, M.J.; Tan, C.C.; Maddar, F.M.; Remy, G.; Abbott, M.; Dixon, S.; McMahon, R.; Curnick, O.; Ellis, M.; Lain, M.; Barai, A.; Amor-Segan, M.; Bhagat, R.; Greenwood, D.; ACS Energy Letters (April 2019) https://doi.org/10.1021/acsenergylett.9b00663 
  10. Advanced Spectroelectrochemical Techniques to Study Electrode Interfaces Within Lithium-Ion and Lithium-Oxygen Batteries; Cowan, A.J.; Hardwick, L.J.; Annual Review of Analytical Chemistry (April 2019) https://doi.org/10.1146/annurev-anchem-061318-115303 (See also SOLBAT)  
  11. Morphology-Directed Synthesis of LiFePO4 and LiCoPO4 from Nanostructured Li1+2 xPO3+ x; El-Shinawi, H.; Cussen, E.J.; Corr, S.A.; Inorganic Chemistry (May 2019) https://doi.org/10.1021/acs.inorgchem.9b00517  
  12. Porous Metal-Organic Frameworks for Enhanced Performance Silicon Anodes in Lithium-Ion Batteries; Malik, R.; Loveridge, M.J.; Williams, L.J.; Huang, Q.; West, G.; Shearing, P.R.; Bhagat, R.; Walton, R.I.; Chemistry of Materials (May 2019) https://doi.org/10.1021/acs.chemmater.9b00933  
  13. Spatially Resolving Lithiation in Silicon-Graphite Composite Electrodes via in Situ High-Energy X-ray Diffraction Computed Tomography; Finegan, D.P.; Vamvakeros, A.; Cao, L.; Tan, C.; Heenan, T.M.M.; Daemi, S.R.; Jacques, S.D.M.; Beale, A.M.; Di Michiel, M.; Smith, K.; Brett, D.J.L.; Shearing, P.R.; Ban, C.; Nano Letters (May 2019) https://doi.org/10.1021/acs.nanolett.9b00955  
  14. Concentrated electrolytes for enhanced stability of Al-alloy negative electrodes in Li-ion batteries; Chan, A.K.; Tatara, R.; Feng, S.; Karayaylali, P.; Lopez, J.; Stephens, I.E.L.; Shao-Horn, Y.; Journal of the Electrochemical Society (June 2019) https://doi.org/10.1149/2.0581910jes  
  15. Electron Paramagnetic Resonance as a Structural Tool to Study Graphene Oxide: Potential Dependence of the EPR Response; Wang, B.; Fielding, A.J.; Dryfe, R.A.W.; Journal of Physical Chemistry C (Aug 2019) https://doi.org/10.1021/acs.jpcc.9b04292 
  16. Virtual unrolling of spirally-wound lithium-ion cells for correlative degradation studies and predictive fault detection; Kok, M.D.R.; Robinson, J.B.; Weaving, J.S.; Jnawali, A.; Pham, M.; Iacoviello, F.; Brett, D.J.L.; Shearing, P.R.; Sustainable Energy and Fuels (Aug 2019) https://doi.org/10.1039/c9se00500e (See also MSM) 
  17. Kerr gated Raman spectroscopy of LiPF6 salt and LiPF6-based organic carbonate electrolyte for Li-ion batteries; Cabo-Fernandez, L.; Neale, A.R.; Braga, F.; Sazanovich, I.V.; Kostecki, R.; Hardwick, L.J.; Physical Chemistry Chemical Physics (Sept 2019) https://doi.org/10.1039/c9cp02430a  
  18. Representative resolution analysis for X-ray CT: A Solid oxide fuel cell case study; Heenan, T.M.M.; Tan, C.; Jervis, R.; Lu, X.; Brett, D.J.L.; Shearing, P.R.; Chemical Engineering Science: X (Nov 2019) https://doi.org/10.1016/j.cesx.2019.100043  
  19. Developments in X-ray tomography characterization for electrochemical devices; Heenan, T.M.M.; Tan, C.; Hack, J.; Brett, D.J.L.; Shearing, P.R.; Materials Today (Dec 2019) https://doi.org/10.1016/j.mattod.2019.05.019  
  20. Intercalation behaviour of Li and Na into 3-layer and multilayer MoS2 flakes; Zou, J.; Li, F.; Bissett, M.A.; Kim, F.; Hardwick, L.J.; Electrochimica Acta (Jan 2020) https://doi.org/10.1016/j.electacta.2019.135284  
  21. Spatial quantification of dynamic inter and intra particle crystallographic heterogeneities within lithium ion electrodes; Finegan, D.P.; Vamvakeros, A.; Tan, C.; Heenan, T.M.M.; Daemi, S.R.; Seitzman, N.; Di Michiel, M.; Jacques, S.; Beale, A.M.; Brett, D.J.L.; Shearing, P.R.; Smith, K.; Nature Communications (Jan 2020) https://doi.org/10.1038/s41467-020-14467-x  
  22. 4D imaging of lithium-batteries using correlative neutron and X-ray tomography with a virtual unrolling technique; Ziesche, R.F.; Arlt, T.; Finegan, D.P.; Heenan, T.M.M.; Tengattini, A.; Baum, D.; Kardjilov, N.; Markötter, H.; Manke, I.; Kockelmann, W.; Brett, D.J.L.; Shearing, P.R.; Nature Communications (Feb 2020) https://doi.org/10.1038/s41467-019-13943-3  
  23. Rapid Preparation of Geometrically Optimal Battery Electrode Samples for Nano Scale X-ray Characterisation; Tan, C.; Daemi, S.; Heenan, T.; Iacoviello, F.; Leach, A.S.; Rasha, L.; Jervis, R.; Brett, D.J.L.; Shearing, P.R.; Journal of the Electrochemical Society (April 2020) https://doi.org/10.1149/1945-7111/ab80cd 
  24. 3D microstructure design of lithium-ion battery electrodes assisted by X-ray nano-computed tomography and modelling; Lu, X.; Bertei, A.; Finegan, D.P.; Tan, C.; Daemi, S.R.; Weaving, J.S.; O’Regan, K.B.; Heenan, T.M.M.; Hinds, G.; Kendrick, E.; Brett, D.J.L.; Shearing, P.R.; Nature Communications (April 2020) https://doi.org/10.1038/s41467-020-15811-x  (See also MSM)  
  25. Thermal Runaway of a Li-Ion Battery Studied by Combined ARC and Multi-Length Scale X-ray CT; Patel, D.; Robinson, J.B.; Ball, S.; Brett, D.J.L.; Shearing, P.R.; Journal of the Electrochemical Society (April 2020) https://doi.org/10.1149/1945-7111/ab7fb6 
  26. Emerging X-ray imaging technologies for energy materials; Cao, C.; Toney, M.F.; Sham, T.-K.; Harder, R.; Shearing, P.R.; Xiao, X.; Wang, J.; Materials Today (April 2020) https://doi.org/10.1016/j.mattod.2019.08.011 (See also SOLBAT) 
  27. In situ Electron paramagnetic resonance spectroelectrochemical study of graphene-based supercapacitors: Comparison between chemically reduced graphene oxide and nitrogen-doped reduced graphene oxide; Wang, B.; Likodimos, V.; Fielding, A.J.; Dryfe, R.A.W.; Carbon (April 2020) https://doi.org/10.1016/j.carbon.2019.12.045  
  28. Resolving Li-Ion Battery Electrode Particles Using Rapid Lab-Based X-Ray Nano-Computed Tomography for High-Throughput Quantification; Heenan, T.M.M.; Llewellyn, A.V.; Leach, A.S.; Kok, M.D.R.; Tan, C.; Jervis, R.; Brett, D.J.L.; Shearing, P.R.; Advanced Science (April 2020) https://doi.org/10.1002/advs.202000362  
  29. Identifying degradation patterns of lithium ion batteries from impedance spectroscopy using machine learning; Zhang, Y.; Tang, Q.; Zhang, Y.; Wang, J.; Stimming, U.; Lee, A.A.; Nature Communications (April 2020) https://doi.org/10.1038/s41467-020-15235-7  
  30. Selective NMR observation of the SEI–metal interface by dynamic nuclear polarisation from lithium metal; Hope, M.A.; Rinkel, B.L.D.; Gunnarsdóttir, A.B.; Märker, K.; Menkin, S.; Paul, S.; Sergeyev, I.V.; Grey, C.P.; Nature Communications (May 2020) https://doi.org/10.1038/s41467-020-16114-x  
  31. Quantitative Relationships between Pore Tortuosity, Pore Topology, and Solid Particle Morphology Using a Novel Discrete Particle Size Algorithm; Usseglio-Viretta, F.L.E.; Finegan, D.P.; Colclasure, A.; Heenan, T.M.M.; Abraham, D.; Shearing, P.; Smith, K.; Journal of the Electrochemical Society (June 2020) https://doi.org/10.1149/1945-7111/ab913b 
  32. The Building Blocks of Battery Technology: Using Modified Tower Block Game Sets to Explain and Aid the Understanding of Rechargeable Li-Ion Batteries; Driscoll, E.H.; Hayward, E.C.; Patchett, R.; Anderson, P.A.; Slater, P.R.; Journal of Chemical Education (June 2020) https://doi.org/10.1021/acs.jchemed.0c00282 (See also CATMAT, Nextrode, ReLIB)  
  33. Theoretical transmissions for X-ray computed tomography studies of lithium-ion battery cathodes; Heenan, T.M.M.; Tan, C.; Wade, A.J.; Jervis, R.; Brett, D.J.L.; Shearing, P.R.; Materials and Design (June 2020) https://doi.org/10.1016/j.matdes.2020.108585  
  34. Exploring cycling induced crystallographic change in NMC with X-ray diffraction computed tomography; Daemi, S.R.; Tan, C.; Vamvakeros, A.; Heenan, T.M.M.; Finegan, D.P.; Di Michiel, M.; Beale, A.M.; Cookson, J.; Petrucco, E.; Weaving, J.S.; Jacques, S.; Jervis, R.; Brett, D.J.L.; Shearing, P.R.; Physical Chemistry Chemical Physics (June 2020) https://doi.org/10.1039/d0cp01851a  
  35. Highly Sensitive Operando Pressure Measurements of Li-ion Battery Materials with a Simply Modified Swagelok Cell; Ryall, N.; Garcia-Araez, N.; Journal of the Electrochemical Society (July 2020) https://doi.org/10.1149/1945-7111/ab9e81 
  36. The origin of chemical inhomogeneity in garnet electrolytes and its impact on the electrochemical performance; Brugge, R.H.; Pesci, F.M.; Cavallaro, A.; Sole, C.; Isaacs, M.A.; Kerherve, G.; Weatherup, R.S.; Aguadero, A.; Journal of Materials Chemistry A (July 2020) https://doi.org/10.1039/d0ta04974c (See also Characterisation) 
  37. Operando Electrochemical Atomic Force Microscopy of Solid-Electrolyte Interphase Formation on Graphite Anodes: The Evolution of SEI Morphology and Mechanical Properties; Zhang, Z.; Smith, K.; Jervis, R.; Shearing, P.R.; Miller, T.S.; Brett, D.J.L.; ACS Applied Materials and Interfaces (July 2020) https://doi.org/10.1021/acsami.0c11190  
  38. Electrolyte oxidation pathways in lithium-ion batteries; Rinkel, B.L.D.; Hall, D.S.; Temprano, I.; Grey, C.P.; Journal of the American Chemical Society (July 2020) https://doi.org/10.1021/jacs.0c06363  
  39. In-Situ Raman Spectroscopy of Reaction Products in Optofluidic Hollow-Core Fiber Microreactors; Gentleman, A.S.; Miele, E.; Lawson, T.; Kohler, P.; Kim, S.; Yousaf, S.; Garcia, D.A.; Lage, A.; Grey, C.P.; Baumberg, J.J.; Frosz, M.H.; Russell, P.S.J.; Reisner, E.; Euser, T.G.; 2020 Conference on Lasers and Electro-Optics Pacific Rim, CLEO-PR 2020 – Proceedings (Aug 2020) https://doi.org/10.1364/CLEOPR.2020.C2H_2  
  40. Erratum: Investigating the effect of a fluoroethylene carbonate additive on lithium deposition and the solid electrolyte interphase in lithium metal batteries usingin situNMR spectroscopy (J. Mater. Chem. A (2020) 8 (14975-14992) DOI: 10.1039/D0TA05652A); Gunnarsdóttir, A.B.; Vema, S.; Menkin, S.; Marbella, L.E.; Grey, C.P.; Journal of Materials Chemistry A (Aug 2020) https://doi.org/10.1039/d0ta90183k  
  41. Bulk fatigue induced by surface reconstruction in layered Ni-rich cathodes for Li-ion batteries; Xu, C.; Märker, K.; Lee, J.; Mahadevegowda, A.; Reeves, P.J.; Day, S.J.; Groh, M.F.; Emge, S.P.; Ducati, C.; Layla Mehdi, B.; Tang, C.C.; Grey, C.P.; Nature Materials (Aug 2020) https://doi.org/10.1038/s41563-020-0767-8  
  42. Correlative acoustic time-of-flight spectroscopy and X-ray imaging to investigate gas-induced delamination in lithium-ion pouch cells during thermal runaway; Pham, M.T.M.; Darst, J.J.; Finegan, D.P.; Robinson, J.B.; Heenan, T.M.M.; Kok, M.D.R.; Iacoviello, F.; Owen, R.; Walker, W.Q.; Magdysyuk, O.V.; Connolley, T.; Darcy, E.; Hinds, G.; Brett, D.J.L.; Shearing, P.R.; Journal of Power Sources (Sept 2020) https://doi.org/10.1016/j.jpowsour.2020.228039  
  43. Operando NMR of NMC811/Graphite Lithium-Ion Batteries: Structure, Dynamics, and Lithium Metal Deposition; Märker, K.; Xu, C.; Grey, C.P.; Journal of the American Chemical Society (Sept 2020) https://doi.org/10.1021/jacs.0c06727  
  44. Ageing analysis and asymmetric stress considerations for small format cylindrical cells for wearable electronic devices; Tan, C.C.; Walker, M.; Remy, G.; Kourra, N.; Maddar, F.; Dixon, S.; Williams, M.; Loveridge, M.J.; Journal of Power Sources (Oct 2020) https://doi.org/10.1016/j.jpowsour.2020.228626  
  45. Data for an Advanced Microstructural and Electrochemical Datasheet on 18650 Li-ion Batteries with Nickel-Rich NMC811 Cathodes and Graphite-Silicon Anodes; Heenan, T.M.M.; Jnawali, A.; Kok, M.; Tranter, T.G.; Tan, C.; Dimitrijevic, A.; Jervis, R.; Brett, D.J.L.; Shearing, P.R.; Data in Brief (Oct 2020) https://doi.org/10.1016/j.dib.2020.106033 
  46. Minimising damage in high resolution scanning transmission electron microscope images of nanoscale structures and processes; Nicholls, D.; Lee, J.; Amari, H.; Stevens, A.J.; Mehdi, B.L.; Browning, N.D.; Nanoscale (Oct 2020) https://doi.org/10.1039/d0nr04589f (See also ReLIB, Characterisation) 
  47. Synthesis of layered silicon-graphene hetero-structures by wet jet milling for high capacity anodes in Li-ion batteries; Malik, R.; Huang, Q.; Silvestri, L.; Liu, D.; Pellegrini, V.; Marasco, L.; Venezia, E.; Abouali, S.; Bonaccorso, F.; Lain, M.J.; Greenwood, D.; West, G.; Shearing, P.R.; Loveridge, M.J.; 2D Materials (Oct 2020) https://doi.org/10.1088/2053-1583/aba5ca  
  48. An advanced microstructural and electrochemical datasheet on 18650 li-ion batteries with nickel-rich NMC811 cathodes and graphite-silicon anodes; Heenan, T.M.M.; Jnawali, A.; Kok, M.D.R.; Tranter, T.G.; Tan, C.; Dimitrijevic, A.; Jervis, R.; Brett, D.J.L.; Shearing, P.R.; Journal of the Electrochemical Society (Nov 2020) https://doi.org/10.1149/1945-7111/abc4c1  
  49. Effect of Anode Slippage on Cathode Cutoff Potential and Degradation Mechanisms in Ni-Rich Li-Ion Batteries; Dose, W.M.; Xu, C.; Grey, C.P.; De Volder, M.F.L.; Cell Reports Physical Science (Nov 2020) https://doi.org/10.1016/j.xcrp.2020.100253  
  50. Identifying the Origins of Microstructural Defects Such as Cracking within Ni-Rich NMC811 Cathode Particles for Lithium-Ion Batteries; Heenan, T.M.M.; Wade, A.; Tan, C.; Parker, J.E.; Matras, D.; Leach, A.S.; Robinson, J.B.; Llewellyn, A.; Dimitrijevic, A.; Jervis, R.; Quinn, P.D.; Brett, D.J.L.; Shearing, P.R.; Advanced Energy Materials (Dec 2020) https://doi.org/10.1002/aenm.202002655 (See also MSM) 
  51. Prospects for lithium-ion batteries and beyond—a 2030 vision; Grey, C.P.; Hall, D.S.; Nature Communications (Dec 2020) https://doi.org/10.1038/s41467-020-19991-4  
  52. Sample Dependence of Magnetism in the Next-Generation Cathode Material LiNi0.8Mn0.1Co0.1O2; Mukherjee, P.; Paddison, J.A.M.; Xu, C.; Ruff, Z.; Wildes, A.R.; Keen, D.A.; Smith, R.I.; Grey, C.P.; Dutton, S.E.; Inorganic Chemistry (Dec 2020) https://doi.org/10.1021/acs.inorgchem.0c02899  
  53. Phase Behavior during Electrochemical Cycling of Ni-Rich Cathode Materials for Li-Ion Batteries; Xu, C.; Reeves, P.J.; Jacquet, Q.; Grey, C.P.; Advanced Energy Materials (Dec 2020) https://doi.org/10.1002/aenm.202003404  
  54. A dilatometric study of graphite electrodes during cycling with x-ray computed tomography; Michael, H.; Iacoviello, F.; Heenan, T.M.M.; Llewellyn, A.; Weaving, J.S.; Jervis, R.; Brett, D.J.L.; Shearing, P.R.; Journal of the Electrochemical Society (Jan 2021) https://doi.org/10.1149/1945-7111/abd648  
  55. The effects of ambient storage conditions on the structural and electrochemical properties of NMC-811 cathodes for Li-ion batteries; Busà, C.; Belekoukia, M.; Loveridge, M.J.; Electrochimica Acta (Jan 2021) https://doi.org/10.1016/j.electacta.2020.137358 
  56. Controlling radiolysis chemistry on the nanoscale in liquid cell scanning transmission electron microscopy; Lee, J.; Nicholls, D.; Browning, N.D.; Mehdi, B.L.; Physical Chemistry Chemical Physics (March 2021) https://doi.org/10.1039/d0cp06369j (See also ReLIB, Characterisation) 
  57. Developments in Dilatometry for Characterisation of Electrochemical Devices; Michael, H.; Jervis, R.; Brett, D.J.L; Shearing, P.R.; Batteries and Supercaps (April 2021) https://doi.org/10.1002/batt.202100027 (See also LiSTAR)  
  58. Operando Measurement of Layer Breathing Modes in Lithiated Graphite; Yadegari, H.; Koronfel, M.A.; Wang, K.; Thornton, D.B.; Stephens, I.E.L.; Molteni, C.; Haynes, P.D.; Ryan, M.P.; ACS Energy Letters (April 2021) https://doi.org/10.1021/acsenergylett.1c00494 
  59. Asphericity Can Cause Nonuniform Lithium Intercalation in Battery Active Particles; Mistry, A.; Heenan, T.; Smith, K.; Shearing, P.; Mukherjee, P.P.; ACS Energy Letters (May 2021) https://doi.org/10.1021/acsenergylett.2c00870 (See also SafeBatt) 
  60. Transition metal dissolution and degradation in nmc811-graphite electrochemical cells; Ruff, Z.; Xu, C.; Grey, C.P.; Journal of the Electrochemical Society (June 2021) https://doi.org/10.1149/1945-7111/ac0359  
  61. Is lithium the key for nitrogen electroreduction?; Westhead, O.; Jervis, R.; Stephens, I.E.L.; Science (June 2021) https://doi.org/10.1126/science.abi8329 
  62. Dendrite suppression by anode polishing in zinc-ion batteries; Zhang, Z.; Said, S.; Smith, K.; Zhang, Y.S.; He, G.; Jervis, R.; Shearing, P.R.; Miller, T.S.; Brett, D.J.L.; Journal of Materials Chemistry A (June 2021) https://doi.org/10.1039/d1ta02682h (See also LiSTAR) 
  63. The Complex Role of Aluminium Contamination in Nickel-Rich Layered Oxide Cathodes for Lithium-Ion Batteries; Lee, J.; Amari, H.; Bahri, M.; Shen, Z.; Xu, C.; Ruff, Z.; Grey, C.P.; Ersen, O.; Aguadero, A.; Browning, N.D.; Mehdi, B.L.; Batteries and Supercaps (June 2021) https://doi.org/10.1002/batt.202100110 (See also ReLIB) 
  64. Degradation in lithium ion battery current collectors; Guo, L.; Thornton, D.B.; Koronfel, M.A.; Stephens, I.E.L.; Ryan, M.P.; JPhys Energy (July 2021) https://doi.org/10.1088/2515-7655/ac0c04  
  65. Toward an Understanding of SEI Formation and Lithium Plating on Copper in Anode-Free Batteries; Menkin, S.; Okeefe, C.A.; Gunnarsdóttir, A.B.; Dey, S.; Pesci, F.M.; Shen, Z.; Aguadero, A.; Grey, C.P.; Journal of Physical Chemistry C (July 2021) https://doi.org/10.1021/acs.jpcc.1c03877 
  66. Characterizing Batteries by In Situ Electrochemical Atomic Force Microscopy: A Critical Review; Zhang, Z.; Said, S.; Smith, K.; Jervis, R.; Howard, C.A.; Shearing, P.R.; Brett, D.J.L.; Miller, T.S.; Advanced Energy Materials (Sept 2021) https://doi.org/10.1002/aenm.202101518 (See also LiSTAR) 
  67. 3D X-ray characterization of energy storage and conversion devices; Tan, C.; Leach, A.S.; Heenan, T.M.M.; Jervis, R.; Brett, D.J.L.; Shearing, P.R.; Advances in Sustainable Energy: Policy, Materials and Devices (Sept 2021) https://doi.org/10.1007/978-3-030-74406-9_18 (See also SOLBAT) 
  68. The influence of electrochemical cycling protocols on capacity loss in nickel-rich lithium-ion batteries; Dose, W.M.; Morzy, J.K.; Mahadevegowda, A.; Ducati, C.; Grey, C.P.; De Volder, M.F.L.; Journal of Materials Chemistry A (Oct 2021) https://doi.org/10.1039/d1ta06324c 
  69. Nanoscale state-of-charge heterogeneities within polycrystalline nickel-rich layered oxide cathode materials; Tan, C.; Leach, A.S.; Heenan, T.M.M.; Parks, H.; Jervis, R.; Weker, J.N.; Brett, D.J.L.; Shearing, P.R.; Cell Reports Physical Science (Dec 2021) https://doi.org/10.1016/j.xcrp.2021.100647 (See also SafeBatt, ReLIB) 
  70. Negating the Interfacial Resistance between Solid and Liquid Electrolytes for Next-Generation Lithium Batteries; Vivek, J.P.; Meddings, N.; Garcia-Araez, N.; ACS Applied Materials and Interfaces (Dec 2021) https://doi.org/10.1021/acsami.1c17247  
  71. Chapter 6 Electron microscopies for batteries; Li, W.; Browning, N.D.; Mehdi, B.L.; Batteries: materials principles and characterization methods (Dec 2021) https://iopscience.iop.org/book/edit/978-0-7503-2682-7/chapter/bk978-0-7503-2682-7ch6  
  72. A solution-processable near-infrared thermally activated delayed fluorescent dye with a fused aromatic acceptor and aggregation induced emission behavior; Congrave, D.G.; Drummond, B.H.; Gu, Q.; Montanaro, S.; Francis, H.; Riesgo-González, V.; Zeng, W.; Matthews, C.S.B.; Dowland, S.; Wright, I.A.; Grey, C.P.; Friend, R.H.; Bronstein, H.; Journal of Materials Chemistry C (Jan 2022) https://doi.org/10.1039/d1tc04753a 
  73. Spatially resolved operando synchrotron-based X-ray diffraction measurements of Ni-rich cathodes for Li-ion batteries; A.S. Leach, A.V. Llewellyn, C. Xu, C. Tan, T.M.M. Heenan, A. Dimitrijevic, K. Kleiner, C.P Grey, D.J.L. Brett, C.C. Tang, P.R. Shearing; R. Jervis; Frontiers in Chemical Engineering (Jan 2022) https://doi.org/10.3389/fceng.2021.794194 (See also SafeBatt)  
  74. In-situ X-ray tomographic imaging study of gas and structural evolution in a commercial Li-ion pouch cell; Du, W.; Owen, R.E.; Jnawali, A.; Neville, T.P.; Iacoviello, F.; Zhang, Z.; Liatard, S.; Brett, D.J.L.; Shearing, P.R.; Journal of Power Sources (Feb 2022) https://doi.org/10.1016/j.jpowsour.2021.230818 (See also SafeBatt, LiSTAR) 
  75. Thermal Runaway of Li-Ion Cells: How Internal Dynamics, Mass Ejection, and Heat Vary with Cell Geometry and Abuse Type; Sharp, M.; Darst, J.J.; Hughes, P.; Billman, J.; Pham, M.; Petrushenko, D.; Heenan, T.M.M.; Jervis, R.; Owen, R.; Patel, D.; Wenjia, D.; Michael, H.; Rack, A.; Magdysyuk, O.V.; Connolley, T.; Brett, D.J.L.; Hinds, G.; Keyser, M.; Darcy, E.; Shearing, P.R.; Walker, W.; Finegan, D.P.; Journal of the Electrochemical Society (Feb 2022) https://doi.org/10.1149/1945-7111/ac4fef (See also SafeBatt) 
  76. Cycle-Induced Interfacial Degradation and Transition-Metal Cross-Over in LiNi0.8Mn0.1Co0.1O2-Graphite Cells; Björklund, E.; Xu, C.; Dose, W.M.; Sole, C.G.; Thakur, P.K.; Lee, T.-L.; De Volder, M.F.L.; Grey, C.P.; Weatherup, R.S.; Chemistry of Materials (Feb 2022) https://doi.org/10.1021/acs.chemmater.1c02722 
  77. Electrolyte Reactivity at the Charged Ni-Rich Cathode Interface and Degradation in Li-Ion Batteries; Dose, W.M.; Temprano, I.; Allen, J.P.; Björklund, E.; O’Keefe, C.A.; Li, W.; Mehdi, B.L.; Weatherup, R.S.; De Volder, M.F.L.; Grey, C.P.; ACS Applied Materials and Interfaces (March 2022) https://doi.org/10.1021/acsami.1c22812  
  78. Hollow-core optical fibre sensors for operando Raman spectroscopy investigation of Li-ion battery liquid electrolytes; Miele, E.; Dose, W.M.; Manyakin, I.; Frosz, M.H.; Ruff, Z.; De Volder, M.F.L.; Grey, C.P.; Baumberg, J.J.; Euser, T.G.; Nature Communications (March 2022) https://doi.org/10.1038/s41467-022-29330-4 
  79. Effect of Lithiation upon the Shear Strength of NMC811 Single Crystals; Stallard, J.C.; Vema, S.; Hall, D.S.; Dennis, A.R.; Penrod, M.E.; Grey, C.P.; Deshpande, V.S.; Fleck, N.A.; Journal of the Electrochemical Society (April 2022) https://doi.org/10.1149/1945-7111/ac6244 (See also FutureCat) 
  80. Cracking predictions of lithium-ion battery electrodes by X-ray computed tomography and modelling; Boyce, A.M.; Martínez-Pañeda, E.; Wade, A.; Zhang, Y.S.; Bailey, J.J.; Heenan, T.M.M.; Brett, D.J.L.; Shearing, P.R.; Journal of Power Sources (April 2022) https://doi.org/10.1016/j.jpowsour.2022.231119 (See also MSM, Nextrode, ReLIB) 
  81. Operando Ultrasonic Monitoring of Lithium-Ion Battery Temperature and Behaviour at Different Cycling Rates and under Drive Cycle Conditions; Owen, R.E.; Robinson, J.B.; Weaving, J.S.; Pham, M.T.M.; Tranter, T.G.; Neville, T.P.; Billson, D.; Braglia, M.; Stocker, R.; Tidblad, A.A.; Shearing, P.R.; Brett, D.J.L.; Journal of the Electrochemical Society (April 2022) https://doi.org/10.1149/1945-7111/ac6833 (See also MSM, SafeBatt, LiSTAR, ReLIB) 
  82. A greyscale erosion algorithm for tomography (GREAT) to rapidly detect battery particle defects; Wade, A.; Heenan, T.M.M.; Kok, M.; Tranter, T.; Leach, A.; Tan, C.; Jervis, R.; Brett, D.J.L.; Shearing, P.R.; npj Materials Degradation (May 2022) https://doi.org/10.1038/s41529-022-00255-z (See also MSM) 
  83. Ni-O-redox, oxygen loss and singlet oxygen formation in LiNiO2 cathodes for Li-ion batteries; Genreith-Schriever, A.R.; Banerjee, H.; Grey, C.P.; Morris, A.J.; arXiv (May 2022) https://doi.org/10.48550/arXiv.2205.10462  
  84. Investigating the presence of adsorbed species on Pt steps at low potentials; Rizo, R.; Fernández-Vidal, J.; Hardwick, L.J.; Attard, G.A.; Vidal-Iglesias, F.J.; Climent, V.; Herrero, E.; Feliu, J.M.; Nature Communications (May 2022) https://doi.org/s41467-022-30241-7  
  85. Dynamics of Solid-Electrolyte Interphase Formation on Silicon Electrodes Revealed by Combinatorial Electrochemical Screening; Martín-Yerga, D.; Milan, D.C.; Xu, X.; Fernández-Vidal, J.; Whalley, L.; Cowan, A.J.; Hardwick, L.J.; Unwin, P.R.; Angewandte Chemie – International Edition (June 2022) https://doi.org/10.1002/anie.202207184  
  86. Aerosol Jet Printing as a Versatile Sample Preparation Method for Operando Electrochemical TEM Microdevices; Morzy, J.K.; Sartor, A.; Dose, W.M.; Ou, C.; Kar-Narayan, S.; De Volder, M.F.L.; Ducati, C.; Advanced Materials Interfaces (June 2022) https://doi.org/10.1002/admi.202200530  
  87. Author Correction: Investigating the presence of adsorbed species on Pt steps at low potentials (Nature Communications, (2022), 13, 1, (2550), 10.1038/s41467-022-30241-7); Rizo, R.; Fernández-Vidal, J.; Hardwick, L.J.; Attard, G.A.; Vidal-Iglesias, F.J.; Climent, V.; Herrero, E.; Feliu, J.M.; Nature Communications (June 2022) https://doi.org/10.1038/s41467-022-31404-2  
  88. Two electrolyte decomposition pathways at nickel-rich cathode surfaces in lithium-ion batteries; Rinkel, B.L.D.; Vivek, J.P.; Garcia-Araez, N.; Grey, C.P.; Energy and Environmental Science (July 2022) https://doi.org/10.1039/d1ee04053g 
  89. Quantitative spatiotemporal mapping of thermal runaway propagation rates in lithium-ion cells using cross-correlated Gabor filtering; Radhakrishnan, A.N.P.; Buckwell, M.; Pham, M.; Finegan, D.P.; Rack, A.; Hinds, G.; Brett, D.J.L.; Shearing, P.R.; Energy and Environmental Science (July 2022) https://doi.org/10.1039/d1ee03430h (See also SafeBatt) 
  90. Long-Life and pH-Stable SnO2-Coated Au Nanoparticles for SHINERS; Fernández-Vidal, J.; Gómez-Marín, A.M.; Jones, L.A.H.; Yen, C.-H.; Veal, T.D.; Dhanak, V.R.; Hu, C.-C.; Hardwick, L.J.; Journal of Physical Chemistry C (July 2022) https://doi.org/10.1021/acs.jpcc.2c02432  
  91. Lithium Insertion into Graphitic Carbon Observed via Operando Kerr-Gated Raman Spectroscopy Enables High State of Charge Diagnostics; Neale, A.R.; Milan, D.C.; Braga, F.; Sazanovich, I.V.; Hardwick, L.J.; ACS Energy Letters (July 2022) https://doi.org/10.1021/acsenergylett.2c01120  
  92. Operando monitoring of single-particle kinetic state-of-charge heterogeneities and cracking in high-rate Li-ion anodes; Merryweather, A.J.; Jacquet, Q.; Emge, S.P.; Schnedermann, C.; Rao, A.; Grey, C.P.; Nature Materials (Aug 2022) https://doi.org/10.1038/s41563-022-01324-z 
  93. Correlative electrochemical acoustic time-of-flight spectroscopy and X-ray imaging to monitor the performance of single-crystal and polycrystalline NMC811/Gr lithium-ion batteries; Michael, H.; Owen, R.E.; Robinson, J.B.; Heenan, T.M.M.; Tan, C.; Wade, A.J.; Jervis, R.; Brett, D.J.L.; Shearing, P.R.; Journal of Power Sources (Sept 2022) https://doi.org/10.1016/j.jpowsour.2022.231775 (See also LiSTAR) 
  94. Revealing solid electrolyte interphase formation through interface-sensitive Operando X-ray absorption spectroscopy; Swallow, J.E.N.; Fraser, M.W.; Kneusels, N.-J.H.; Charlton, J.F.; Sole, C.G.; Phelan, C.M.E.; Björklund, E.; Bencok, P.; Escudero, C.; Pérez-Dieste, V.; Grey, C.P.; Nicholls, R.J.; Weatherup, R.S.; Nature Communications (Sept 2022) https://doi.org/10.1038/s41467-022-33691-1 
  95. Surface reduction in lithium- and manganese-rich layered cathodes for lithium ion batteries drives voltage decay; Wen, B.; Sayed, F.N.; Dose, W.M.; Morzy, J.K.; Son, Y.; Nagendran, S.; Ducati, C.; Grey, C.P.; De Volder, M.F.L.; Journal of Materials Chemistry A (Sept 2022) https://doi.org/10.1039/D2TA04876K (See also FutureCat, CATMAT)  
  96. Onset Potential for Electrolyte Oxidation and Ni-Rich Cathode Degradation in Lithium-Ion Batteries; Dose, W.M.; Li, W.; Temprano, I.; O’Keefe, C.A.; Mehdi, B.L.; De Volder, M.F.L.; Grey, C.P.; ACS Energy Letters (Sept 2022) https://doi.org/10.1021/acsenergylett.2c01722  
  97. Giant mid-IR resonant coupling to molecular vibrations in sub-nm gaps of plasmonic multilayer metafilms; Arul, R.; Grys, D.-B.; Chikkaraddy, R.; Mueller, N.S.; Xomalis, A.; Miele, E.; Euser, T.G.; Baumberg, J.J.; Light: Science and Applications (Sept 2022) https://doi.org/10.1038/s41377-022-00943-0  
  98. Operando visualization of kinetically induced lithium heterogeneities in single-particle layered Ni-rich cathodes; Xu, C.; Merryweather, A.J.; Pandurangi, S.S.; Lun, Z.; Hall, D.S.; Deshpande, V.S.; Fleck, N.A.; Schnedermann, C.; Rao, A.; Grey, C.P.; Joule (Oct 2022) https://doi.org/10.1016/j.joule.2022.09.008 
  99. Improving capacity retention at 4.3 V in modified single crystal Ni-rich NMC//graphite pouch cells; Paez Fajardo, G.J.; Belekoukia, M.; Fiamegkou, E.; Menon, A.S.; Ruff, Z.; Shen, Z.; Shah, N.;  Bjorklund, E.; Zuba, M.J.; Lee, T.-L.; Thakur, P.K.; Grey, C.P.; Weatherup, R.; Loveridge, M.; Piper, L.F.P.; SSRN (Oct 2022) https://doi.org/10.2139/ssrn.4255454 (See also SafeBatt) 
  100. Effect of Annealing on the Structure, Composition, and Electrochemistry of NMC811 Coated with Al2O3 Using an Alkoxide Precursor; Riesgo-González, V.; Hall, D.S.; Märker, K.; Slaughter, J.; Wright, D.S.; Grey, C.P.; Chemistry of Materials (Oct 2022) https://doi.org/10.1021/acs.chemmater.2c02580  
  101. Surface Analysis of Pristine and Cycled NMC/Graphite Lithium-Ion Battery Electrodes: Addressing the Measurement Challenges; Marchesini, S.; Reed, B.P.; Jones, H.; Matjacic, L.; Rosser, T.E.; Zhou, Y.; Brennan, B.; Tiddia, M.; Jervis, R.; Loveridge, M.J.; Raccichini, R.; Park, J.; Wain, A.J.; Hinds, G.; Gilmore, I.S.; Shard, A.G.; Pollard, A.J.; ACS Applied Materials and Interfaces (Nov 2022) https://doi.org/10.1021/acsami.2c13636  
  102. Synthesis of Heterometallic Zirconium Alkoxide Single-Source Precursors for Bimetallic Oxide Deposition; Slaughter, J.; Coates, C.; Phillips, G.; Choudhury, D.; Bond, A.D.; Grey, C.P.; Wright, D.S.; Inorganic Chemistry (Nov 2022) https://doi.org/10.1021/acs.inorgchem.2c02852 
  103. Determining the oxidation states of dissolved transition metals in battery electrolytes from solution NMR spectra; Allen, J.P.; Grey, C.P.; Chemical Communications (Jan 2023) https://doi.org/10.1039/D2CC06655F  
  104. Direct 4D Observations of Electrochemically Induced Intergranular Cracking in NMC811 Particles; Parks, H.C.W.; Boyce, A.M.; Wade, A.; Heenan, T.M.M.; Tan, C.; Martínez-Pañeda, E.; Shearing, P.R.; Brett, D.J.L.; Jervis, R.; ChemRxiv (Jan 2023) https://doi.org/10.26434/chemrxiv-2023-h3lzv-v2 
  105. Monitoring the Formation of Nickel-Poor and Nickel-Rich Oxide Cathode Materials for Lithium-Ion Batteries with Synchrotron Radiation; Ying, B.; Fitzpatrick, J.R.; Teng, Z.; Chen, T.; Lo, T.W.B.; Siozios, V.; Murray, C.A.; Brand, H.E.A.; Day, S.; Tang, C.C.; Weatherup, R.S.; Merz, M.; Nagel, P.; Schuppler, S.; Winter, M.; Kleiner, K.; Chemistry of Materials (Jan 2023) https://doi.org/10.1021/acs.chemmater.2c02639 (See also Characterisation) 
  106. The importance of electronic correlations in exploring the exotic phase diagram of layered LixMnO2; Banerjee, H.; Grey, C.P.; Morris, A.J.; Physical Review B (April 2023) https://doi.org/10.1103/PhysRevB.108.165124  
  107. Chemo-Mechanical Analysis of Lithiation/Delithiation of Ni-rich Single Crystals; Pandurangi, S.S.; Hall, D.S.; Grey, C.P.; Deshpande, V.S.; Fleck, N.A.; Journal of the Electrochemical Society (May 2023) https://doi.org/10.1149/1945-7111/acd47e 
  108. Oxygen-redox activity in non-Li-excess W-doped LiNiO2; Menon, A.S.; Johnston, B.J.; Booth, S.G.;Zhang,L.;Kress, K.; Murdock,B.E.;Paez Farjardo, G.; Anthonisamy, N.N.; Tapia-Ruiz, N.; Agrestini, S.; Garcia-Fernandez,M.; Zhou,K.; Thakur, P.K.; Lee, T.L.; Nedoma, A.J.; Cussen, S.A.; Piper, L.F.J.; PRX Energy (March 2023) https://doi.org/10.1103/PRXEnergy.2.013005 (See also FutureCat)  
  109. Shell-isolated nanoparticle-enhanced Raman spectroscopy; Zhang, Y.-J.; Ze, H.; Fang, P.-P.; Huang, Y.-F.; Kudelski, A.; Fernández-Vidal, J.; Hardwick, L.J.; Lipkowski, J.; Tian, Z.-Q.; Li, J.-F.; Nature Reviews Methods Primers (May 2023) https://doi.org/10.1038/s43586-023-00217-y 
  110. Mapping internal temperatures during high-rate battery applications; Heenan, T.M.M.; Mombrini, I.; Llewellyn, A.; Checchia, S.; Tan, C.; Johnson, M.J.; Jnawali, A.; Garbarino, G.; Jervis, R.; Brett, D.J.L.; Di Michiel, M.; Shearing, P.R.; Nature (May 2023) https://doi.org/10.1038/s41586-023-05913-z (See also SafeBatt) 
  111. Direct Observation of Dynamic Lithium Diffusion Behavior in Nickel-Rich, LiNi0.8Mn0.1Co0.1O2 (NMC811) Cathodes Using Operando Muon Spectroscopy; McClelland, I.; Booth, S.G.; Anthonisamy, N.N.; Middlemiss, L.A.; Pérez, G.E.; Cussen, E.J.; Baker, P.J.; Cussen, S.A.; Chemistry of Materials (May 2023) https://doi.org/10.1021/acs.chemmater.2c03834 (See also FutureCat, Nextrode) 
  112. First Cycle Cracking Behaviour Within Ni-Rich Cathodes During High-Voltage Charging; Wade, A.; Llewellyn, A.V.; Heenan, T.M.M.; Tan, C.; Brett, D.J.L.; Jervis, R.; Shearing, P.R.; Journal of the Electrochemical Society (June 2023) https://doi.org/10.1149/1945-7111/ace130  
  113. O3 to O1 Phase Transitions in Highly Delithiated NMC811 at Elevated Temperatures; Ruff, Z.; Coates, C.S.; Märker, K.; Mahadevegowda, A.; Xu, C.; Penrod, M.E.; Ducati, C.; Grey, C.P.; Chemistry of Materials (June 2023) https://doi.org/10.1021/acs.chemmater.3c00307  
  114. Oxygen hole formation controls stability in LiNiO2 cathodes; Genreith-Schriever, A.R.; Banerjee, H.; Menon, A.S.; Bassey, E.N.; Piper, L.F.J.; Grey, C.P.; Morris, A.J.; Joule (July 2023) https://doi.org/10.1016/j.joule.2023.06.017  
  115. Determining the fundamental failure modes in Ni-rich lithium ion battery cathodes; Wang, S.; Shen, Z.; Omirkhan, A.; Gavalda-Diaz, O.; Ryan, M.P.; Giuliani, F.; Journal of the European Ceramic Society (Aug 2023) https://doi.org/10.1016/j.jeurceramsoc.2023.08.021 
  116. Insights into surface chemistry down to nanoscale: An accessible colour hyperspectral imaging approach for scanning electron microscopy; Nohl, J.F.; Farr, N.T.H.; Sun, Y.; Hughes, G.M.; Stehling, N.; Zhang, J.; Longman, F.; Ives, G.; Pokorná, Z.; Mika, F.; Kumar, V.; Mihaylova, L.; Holland, C.; Cussen, S.A.; Rodenburg, C.; Materials Today Advances (Aug 2023) https://doi.org/10.1016/j.mtadv.2023.100413 (See also Nextrode, FutureCat) 
  117. 3D Nanocomposite Thin Film Cathodes for Micro-Batteries with Enhanced High-Rate Electrochemical Performance over Planar Films; Lovett, A.J.; Daramalla, V.; Nayak, D.; Sayed, F.N.; Mahadevegowda, A.; Ducati, C.; Spencer, B.F.; Dutton, S.E.; Grey, C.P.; MacManus-Driscoll, J.L.; Advanced Energy Materials (Aug 2023) https://doi.org/10.1002/aenm.202302053 (See also CATMAT, FutureCat) 
  118. Understanding improved capacity retention at 4.3 V in modified single crystal Ni-rich NMC//graphite pouch cells at elevated temperature; Páez Fajardo, G.J.; Belekoukia, M.; Bolloju, S.; Fiamegkou, E.; Menon, A.S.; Ruff, Z.; Shen, Z.; Shah, N.; Björklund, E.; Zuba, M.J.; Lee, T-L.; Thakur, P.K.; Weatherup, R.S.; Aguadero, A.; Loveridge, M.J.; Grey, C.P.; Piper, L.F.J.; RSC Applied Interfaces (Sept 2023) https://doi.org/10.1039/D3LF00093A 
  119. Direct observations of electrochemically induced intergranular cracking in polycrystalline NMC811 particles; Parks, H.C.W.; Boyce, A.M.; Wade, A.; Heenan, T.M.M.; Tan, C.; Martínez-Pañeda, E.; Shearing, P.R.; Brett, D.J.L.; Jervis, R.; Journal of Materials Chemistry A (Sept 2023) https://doi.org/10.1039/D3TA03057A (See also MSM, Nextrode)  
  120. Elucidating local diffusion dynamics in nickel-rich layered oxide cathodes; Johnston, B.I.J.; McClelland, I.; Baker, P.J.; Cussen, S.A.; Physical Chemistry Chemical Physics (Sept 2023) https://doi.org/10.1039/D3CP02662K (See also FutureCat) 
  121. The strength of a constrained lithium layer; Stallard, J.C.; Vema, S.; Grey, C.P.; Deshpande, V.S.; Fleck, N.A.; Acta Materialia (Sept 2023) https://doi.org/10.1016/j.actamat.2023.119313 (See also FutureCat, SOLBAT) 

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